Using the CIQTEK Scanning NV Microscope (SNVM), the team successfully demonstrated room-temperature ferromagnetism in the semiconducting material MnS₂. The findings were published in the Journal of the American Chemical Society (JACS) under the title “Experimental Evidence of Room-Temperature Ferromagnetism in Semiconducting MnS₂.”

https://pubs.acs.org/doi/10.1021/jacs.5c10107

Pioneering Discovery in 2D Ferromagnetic Semiconductors

The discovery of 2D ferromagnetic semiconductors has raised great expectations for advancing Moore’s Law and spintronics in memory and computation. However, most explored 2D ferromagnetic semiconductors exhibit Curie temperatures far below room temperature. Despite theoretical predictions of many potential room-temperature 2D ferromagnetic materials, the experimental synthesis of ordered and stable metastable structures remains a formidable challenge.

In this study, the researchers developed a template-assisted chemical vapor deposition (CVD) method to synthesize layered MnS₂ microstructures within a ReS₂ template. High-resolution atomic characterizations revealed that the monolayer MnS₂ microstructure crystallized well in a distorted T-phase. The optical bandgap and temperature-dependent carrier mobility confirmed its semiconducting nature.

By combining vibrating sample magnetometry (VSM), electrical transport measurements, and micro-magnetic imaging using CIQTEK SNVM, the team provided solid experimental evidence of room-temperature ferromagnetism in MnS₂. Electrical transport measurements also revealed an anomalous Hall resistance component in the monolayer samples. Theoretical calculations further indicated that this ferromagnetism originates from short-range Mn–Mn interactions.

This work not only confirms the intrinsic room-temperature ferromagnetism of layered MnS₂ but also proposes an innovative approach for the growth of metastable functional 2D materials.

Two Key Breakthroughs

• Intrinsic Room-Temperature Ferromagnetism in MnS₂ Monolayers:
  The study experimentally demonstrates intrinsic room-temperature ferromagnetism in semiconducting MnS₂, resolving the long-standing conflict between semiconductivity and magnetism.

• Template-Assisted CVD Strategy for Metastable Ferromagnetic Microstructures:
  The developed synthesis strategy enables scalable fabrication of metastable ferromagnetic microstructures.

These advances establish MnS₂ as a model platform for 2D spintronics, offering a new pathway for engineering low-dimensional magnetic materials.

ChatGPT 说：

Figure 2: Micro-Region Magnetic Imaging

Figure 3: Electrical Transport Measurements

CIQTEK SNVM: Key Instrument Behind the Discovery

The CIQTEK Scanning NV Microscope (SNVM) played a crucial role in this research. Its high-precision nanoscale magnetic imaging capabilities were essential for visualizing and confirming the magnetic properties of MnS₂. This study highlights how CIQTEK's advanced scientific instruments are empowering frontier research in materials science and condensed matter physics.

This breakthrough not only drives progress in 2D material studies but also opens new opportunities for spintronics and next-generation memory technologies.

Experience CIQTEK SNVM

CIQTEK SNVM is a world-leading nanoscale magnetic field imaging system, offering:

• Temperature range: 1.8–300 K

• Vector magnetic field: 9/1/1 T

• Magnetic spatial resolution: 10 nm

• Magnetic sensitivity: 2 μT/Hz¹ᐟ²

Based on NV center-based optically detected magnetic resonance (ODMR) and atomic force microscopy (AFM) scanning imaging, the SNVM provides high spatial resolution, high magnetic sensitivity, multifunctional detection, and non-invasive measurement.

It is a powerful tool for magnetic domain characterization, antiferromagnetic imaging, superconductivity studies, and 2D magnetic materials research, enabling scientists to explore materials with high precision and confidence.

The 15th China Symposium on Electron Paramagnetic Resonance (EPR) Spectroscopy was successfully held at Chongqing University from October 24 to 27, 2025. Nearly one hundred experts, scholars, industry representatives, and graduate students gathered to discuss cutting-edge topics in the EPR field, including new techniques and theories, biological spin labeling, and new energy applications.

Grand Launch: CIQTEK Q-Band EPR Spectrometers Make a Stunning Debut

As a pioneer in paramagnetic resonance technology, CIQTEK officially unveiled its new Q-band EPR spectrometer series — the EPR-Q400 High-Frequency Pulse Spectrometer and the EPR-Q300 Continuous-Wave Spectrometer, marking another significant milestone in high-frequency EPR technology.

Compared with traditional X-band EPR, high-frequency EPR offers:

• Higher spectral resolution

• Stronger orientation selectivity

• Enhanced sensitivity

Making it a powerful tool for biomacromolecular structure studies, spin dynamics research, and materials science applications.

Dr. Richard Shi from CIQTEK Introduces the New Q-Band EPR Instruments at the Meeting

Flagship Model: EPR-Q400 High-Frequency Pulse Spectrometer

The EPR-Q400, the flagship model of this release, supports both CW and pulsed EPR measurements, meeting a wide range of research demands. It enables variable-temperature experiments from 4 K to 300 K, providing flexible and precise experimental conditions.

Notably, the Q-band spectrometer adopts the same software platform as CIQTEK X-band EPR systems, greatly reducing the learning curve and ensuring a seamless and user-friendly operation experience.

Dedicated CW Solution: EPR-Q300 Continuous-Wave Spectrometer

For users focusing solely on continuous-wave EPR experiments, CIQTEK introduced the EPR-Q300, offering a targeted and efficient solution for diverse scientific applications.

Continuous Innovation in EPR Technology

This product launch showcases CIQTEK’s robust R&D capabilities and in-depth technical expertise in EPR spectroscopy, thereby further enriching its EPR product portfolio. During the symposium, multiple experts recognized CIQTEK’s responsive and professional technical support, noting that the team not only helps resolve experimental challenges but also actively participates in collaborative research, contributing to high-level scientific achievements.

Upcoming Event: CIQTEK Paramagnetic Academy 2026

To further promote academic exchange and talent development in EPR technology, the CIQTEK Paramagnetic Academy Advanced EPR Workshop will be held from July 17 to 27, 2026, in conjunction with the CIQTEK EPR User Symposium.

These events will serve as an open platform for technical communication, experience sharing, and application discussions among EPR researchers and users.
Stay tuned for more updates and upcoming event announcements.

The Center for Micro/Nanoscale Behavior of Materials at Xi’an Jiaotong University (XJTU) has established a comprehensive in-situ materials performance research platform based on the CIQTEK SEM4000 Field Emission Scanning Electron Microscope (FE-SEM). By integrating multiple in-situ testing systems, the center has achieved remarkable progress in the application of in-situ SEM techniques and advanced materials science research.

Leading national research infrastructure

The XJTU Center for Micro/Nanoscale Behavior of Materials focuses on the structure–property relationship of materials at the micro/nanoscale. Since its establishment, the center has published over 410 high-impact papers, including in Nature and Science, demonstrating outstanding scientific output.

The center houses one of the most advanced in-situ materials performance research platforms in China, equipped with large-scale systems such as a Hitachi 300 kV environmental TEM with quantitative nanomechanical–thermal coupling capabilities and an environmental aberration-corrected TEM for atomic-scale in-situ studies of thermo-mechanical-gas interactions. Together, these instruments provide powerful technical support for frontier materials research.

Efficient and seamless experience with CIQTEK SEM

In 2024, the center introduced the CIQTEK SEM4000 Field Emission Scanning Electron Microscope.
Dr. Fan Chuanwei, equipment manager at the center, remarked:

“The resolution and stability of the CIQTEK SEM4000 perfectly meet our research demands. What impressed us most was the efficiency. It took less than four months from equipment installation to our first paper published using the system, and the entire process from procurement to operation and after-sales was highly efficient.”

Regarding customized services, Dr. Fan added:

“For our in-situ SEM experiments, CIQTEK tailored a real-time video recording module and designed customized adapter stages for various in-situ setups. The rapid response and flexibility of the CIQTEK team fully demonstrate their professional expertise.”

Integrated in-situ testing capabilities

The SEM4000 platform at XJTU has successfully integrated three core in-situ testing systems, forming a complete in-situ mechanical performance research capability.

• Bruker Hysitron PI 89 Nanomechanical Test System – Enables nanoindentation, tensile, fracture, fatigue, and mechanical property mapping. It has been extensively used in micro/nanoscale mechanical testing of semiconductor devices, leading to significant results in semiconductor materials research.

• KW In-situ Tensile Stage – Offers a loading range from 1 N to 5 kN and supports various grips, including standard compression/tension, compact tension, three-point bending, and fiber tensile testing. Combined with SEM imaging, it allows real-time correlation of mechanical data with microstructural evolution, providing critical insights into deformation mechanisms.

• Custom In-situ Torsion Stage – Developed by Prof. Wei Xueyong’s team at the School of Instrument Science and Engineering, XJTU, this system enables torsional deformation studies under SEM observation, adding a unique capability to the research platform.

CIQTEK Field Emission SEM4000 at Xi'an Jiaotong University

Dr. Fan commented:

“The systems are well integrated with the SEM and easy to operate. Our researchers quickly became proficient, and these combined techniques have provided a wealth of valuable experimental data and scientific discoveries.”

SEM4000: Designed for in-situ excellence

The outstanding performance of SEM4000 in in-situ studies benefits from its purpose-built engineering design. According to CIQTEK engineers, the large chamber and long-travel stage provide ample space and stability for complex in-situ setups, which is a key advantage over conventional SEMs.

Its modular architecture, featuring 16 flange interfaces, allows flexible customization of vacuum ports and electrical feedthroughs for different in-situ devices. This design makes integration and system expansion remarkably straightforward.

In addition, the integrated in-situ video recording function enables continuous observation and recording of microstructural evolution during experiments, providing crucial data for dynamic process analysis and mechanism exploration.

Continuous innovation for future research

Looking ahead, the XJTU center plans several technology development initiatives based on the SEM4000 platform, reflecting strong confidence in the long-term advancement of CIQTEK scientific instruments.

“We plan to add in-situ heating and EBSD modules for high-temperature and EBSD observations. We also aim to extend our self-developed quantitative in-situ mechanical analysis software, which was originally developed for TEM, to SEM applications. Furthermore, we’re developing an ‘SEM AI Agent’ system to enable automated operation, image acquisition, and data processing through AI assistance,” said Dr. Fan.

“With these continuous improvements, we hope to achieve more breakthroughs in understanding micro/nanoscale material behavior while contributing to the progress and broader adoption of advanced domestic scientific instruments. With CIQTEK’s support, we are confident in realizing these goals.”

The collaboration between Xi'an Jiaotong University and CIQTEK demonstrates the strong potential and technological depth of CIQTEK's high-end scientific instruments in frontier research. From the first paper produced within four months to the successful integration of multiple in-situ testing systems, the CIQTEK SEM4000 has proven to be a cornerstone of XJTU’s advanced materials research platform, earning recognition from one of the nation’s leading research institutions.

A research team led by Prof. Haomin Wang from the Shanghai Institute of Microsystem and Information Technology, Chinese Academy of Sciences, has achieved significant progress in studying the magnetism of zigzag graphene nanoribbons (zGNRs) using the CIQTEK Scanning NV Microscope (SNVM).

Building on their previous research, the team fabricated oriented atomic grooves in hexagonal boron nitride (hBN) by pre-etching with metal nanoparticles and synthesized chiral-controlled graphene nanoribbons within these grooves through a vapor-phase catalytic CVD method. The resulting ~9 nm-wide zGNRs embedded in the hBN lattice exhibited intrinsic magnetic properties, which were directly confirmed experimentally for the first time using SNVM combined with magnetic transport measurements.

This groundbreaking work lays a solid foundation for developing graphene-based spintronic devices. The study, titled “Signatures of magnetism in zigzag graphene nanoribbons embedded in a hexagonal boron nitride lattice”, was published in the renowned journal Nature Materials.

https://doi.org/10.1038/s41563-025-02317-4

Understanding Graphene Magnetism

Graphene, as a unique two-dimensional material, exhibits p-orbital electron magnetism that differs fundamentally from the localized d/f orbital magnetism found in conventional materials. This distinction opens new directions for exploring carbon-based quantum magnetism. Zigzag graphene nanoribbons (zGNRs) are particularly promising for spintronic applications because of their predicted magnetic electronic states near the Fermi level. However, detecting zGNR magnetism through electrical transport measurements has remained highly challenging.

The main difficulties include the limited length of bottom-up synthesized nanoribbons, which complicates device fabrication, and the chemically reactive edges that lead to instability or inhomogeneous doping. Furthermore, in narrow zGNRs, strong antiferromagnetic coupling between edge states makes it difficult to electrically detect magnetic signals. These challenges have hindered direct observation of intrinsic magnetism in zGNRs.

SNVM Reveals Magnetic Signals at Room Temperature

Embedding zGNRs within an hBN lattice enhances edge stability and introduces built-in electric fields, providing an ideal environment for studying magnetism. Using CIQTEK’s room-temperature SNVM, the researchers directly visualized magnetic signals in zGNRs for the first time under ambient conditions.

Figure 1. Magnetic measurement of zGNRs embedded in a hexagonal boron nitride lattice using the Scanning NV Microscope

In electrical transport measurements, the ~9 nm-wide zGNR transistors demonstrated high conductivity and ballistic transport behavior. Under magnetic fields, the devices showed pronounced anisotropic magnetoresistance, with resistance changes up to 175 Ω and a magnetoresistance ratio of approximately 1.3% at 4 K, which persisted up to 350 K. Magnetic hysteresis appeared only when the magnetic field was applied perpendicular to the zGNR plane, confirming magnetic anisotropy. Analysis of the angular dependence of magnetoresistance indicated that the magnetic moments were oriented normal to the sample surface. The decrease in magnetoresistance with increasing source-drain bias and temperature revealed interactions between magnetic response, charge transport, and thermal vibrations.

By combining SNVM imaging with transport characterization, this study provides the first direct evidence of intrinsic magnetism in zGNRs embedded in hBN and demonstrates the potential for electric-field control of magnetic behavior. This work deepens the understanding of graphene magnetism and opens new opportunities for developing graphene-based spintronic devices.

Experience Nanoscale Magnetic Imaging with CIQTEK SNVM

CIQTEK invites researchers to experience the Scanning NV Microscope (SNVM), a world-leading nanoscale magnetic imaging system featuring a temperature range of 1.8–300 K, a 9/1/1 T vector magnetic field, 10 nm magnetic spatial resolution, and 2 μT/Hz¹ᐟ² magnetic sensitivity.

CIQTEK SNVM: the ambient version and the cryogenic version

The SNVM integrates diamond nitrogen-vacancy (NV) center-based optically detected magnetic resonance (ODMR) with atomic force microscopy (AFM) scanning technology. It offers high spatial resolution, superior magnetic sensitivity, multifunctional detection, and non-invasive imaging capabilities, making it an essential tool for research in magnetic domain characterization, antiferromagnetic imaging, superconductivity studies, and two-dimensional magnetic materials.

CIQTEK continues to expand its presence in Europe with the establishment of an SEM demo station in Spain, operated by the trusted local distributor IESMAT. Located in Madrid, the demo station features a CIQTEK High-Performance and Universal Tungsten Filament SEM Microscope SEM3200, providing Spanish users with convenient access to live demonstrations, sample testing, and hands-on operation. The facility also offers professional Spanish-language service and technical consultation, helping local customers better understand and apply CIQTEK’s advanced electron microscopy technologies.

Since the installation of the CIQTEK SEM3200, IESMAT has actively organized a series of seminars and workshops throughout 2025, typically held every one to two months. These events welcome researchers and professionals from academia and industry to explore the performance and advantages of CIQTEK scanning electron microscopes through hands-on sessions and interactive learning experiences.

IESMAT SEM Workshop in January 2025

IESMAT SEM Seminar in Feb, 2025

IESMAT Most Recent SEM Seminar in Sep, 2025

The next event, IESMAT Electron Microscopy Day II, will take place on November 6, 2025, in Madrid. Participants will enjoy:

• Live hands-on electron microscopy with the CIQTEK SEM3200

• Cutting-edge analytics using EDS and EBSD

• Insights into current trends and future directions of electron microscopy in Spain

The SEM demo station at IESMAT marks an important milestone in CIQTEK’s European development strategy. It enhances local accessibility to advanced electron microscopy technologies and provides researchers with authentic, real-world experience. Through close collaboration with partners like IESMAT, CIQTEK is deepening its engagement with the European market, promoting innovation, and building stronger connections with the scientific community.

CIQTEK remains committed to empowering global users through advanced instrumentation, localized service, and continuous collaboration for scientific progress.

The CIQTEK Electron Microscope Factory serves as the company’s dedicated manufacturing and training center for electron microscopy systems. Equipped with advanced production facilities, precision assembly lines, and demonstration laboratories, the factory integrates R&D, manufacturing, quality control, and user training to ensure high performance and reliability across CIQTEK SEM, FIB-SEM, and TEM product lines.

The training was hosted by Mr. Gao, Head of the Electron Microscopy Solutions Department at CIQTEK, together with senior engineers from the CIQTEK electron microscopy team. During the program, participants received systematic instruction on key procedures such as ion pump baking, aperture position inspection, filament centering, high-resolution imaging practice, and accessory installation and calibration.

Throughout the week, the GSEM team worked closely with CIQTEK engineers to gain both theoretical and practical understanding of CIQTEK’s electron microscopy technology. The sessions were designed to ensure that GSEM’s sales and service engineers are fully equipped with the technical expertise required to support local customers in Korea, from system installation and operation to advanced troubleshooting and maintenance.

This training not only enhanced GSEM’s technical capabilities but also strengthened the partnership between CIQTEK and GSEM. With continuous collaboration in product knowledge, application support, and customer service, CIQTEK and GSEM will jointly provide more professional, efficient, and reliable solutions to the Korean electron microscopy market.

CIQTEK remains committed to empowering global partners through professional training, technical collaboration, and continuous innovation in scientific instrumentation.

CIQTEK has achieved a global milestone by completing the world’s first EPR spectrometer modernization project at Queen Mary University of London. The successful upgrade demonstrates CIQTEK’s strong technical expertise and dedication to providing efficient, high-quality services for researchers worldwide.

The project took place at Queen Mary University of London, within the School of Physical and Chemical Sciences, where the EPR research group had long relied on an aging EPR spectrometer. Over time, their system could no longer meet the demands of advanced magnetic resonance studies. Facing this challenge, the team sought a reliable and effective way to enhance their EPR capabilities without fully replacing their existing instrument.

Upon learning about CIQTEK’s comprehensive and industry-leading EPR modernization service, and after in-depth communication with the CIQTEK EPR team, the researchers identified the perfect solution. CIQTEK’s modernization approach provides a cost-effective path to extend the lifetime of existing EPR instruments while significantly improving performance through upgraded hardware, optimized control systems, and advanced functionalities such as continuous-wave (CW) EPR.

EPR Team Preparing the Shipment

In October 2025, CIQTEK’s installation and training engineers delivered a seamless, full-cycle service from shipping and on-site setup to professional user training. The modernization was completed efficiently, enabling the Queen Mary University EPR group to continue their research with a renewed and high-performance system.

CIQTEK and Queen Mary University EPR Teams

Dr. Liu, head of the EPR research team, shared his feedback after the completion of the project:

“This collaboration has far exceeded our expectations. The service efficiency was excellent, the training was thorough and well organized, and we are very satisfied with the test results. We look forward to working with CIQTEK again in the future.”

His comments perfectly reflect CIQTEK’s service principles: “Quality Service. Trusted Partner.”

We would also like to express our sincere gratitude to our UK partner, SciMed, for their valuable local support and coordination throughout the project. Their collaboration ensured smooth communication and timely progress at every stage.

About CIQTEK EPR Modernization Service

CIQTEK EPR Modernization & Upgrade Service gives existing EPR users a second life for their instruments. By replacing outdated control and detection modules with CIQTEK’s state-of-the-art technology, researchers can enjoy enhanced stability, sensitivity, and user experience comparable to new-generation spectrometers while keeping their original system platform. The service supports both continuous-wave and pulse EPR configurations and is compatible with a wide range of legacy models. Learn more about this service here. 

This successful project showcases CIQTEK’s commitment to scientific excellence, customer success, and continuous innovation in the global EPR community.

Looking ahead, CIQTEK will continue expanding its international service network and modernization solutions, empowering more researchers worldwide to revitalize their EPR systems and explore new frontiers in spin science with confidence and creativity.

At ESEM 2025, CIQTEK showcased its SEM product line, including FIBSEM, FESEM, and Tungsten Filament SEM. Our booth drew interest from both biological and materials science researchers, keen to see real-sample imaging, low-voltage performance, and analytical integration.

Beyond exhibits, CIQTEK representatives engaged in technical exchange, discussing how advanced SEM tools can bolster regional research infrastructure. We emphasized our commitment to delivering high-performing instruments, competitive pricing, and local support networks to facilitate adoption in diverse labs across the region.

Impact & Outlook

The conference underscored how microscopy continues to unveil the unseen—from cellular ultrastructure to nanomaterial phenomena. For many participants, this was a rare opportunity to access a wide spectrum of imaging techniques under one roof, and to converse directly with vendors like CIQTEK.

By engaging with local scientists and institutions, CIQTEK deepens its global reach and contributes to the growth of microscopy in underrepresented regions. We look forward to continuing our support in Africa and the Middle East through instrument installations, training, and responsive service.

CIQTEK has taken another important step forward in Europe with the installation of the SEM4000Pro Field Emission Scanning Electron Microscope (FE-SEM) at the SYNERGIE4 demonstration showroom in France.

The new setup allows researchers and industrial users in Europe to experience high-resolution imaging, analytical performance, and ease of operation offered by the CIQTEK SEM4000Pro. The system provides outstanding image quality for fine microstructural observation and supports a wide range of applications in materials science, microelectronics, and R&D.

SYNERGIE4 is CIQTEK's French distributor and service provider for advanced microscopy and microanalysis solutions. With extensive experience in electron microscopy and analytical instruments, SYNERGIE4 supports universities, research institutes, and industrial labs across France with tailored solutions, technical expertise, and training.

Now, SYNERGIE4’s demo center features a fully operational CIQTEK SEM4000Pro, offering hands-on demonstrations for visitors to explore its imaging capabilities, intuitive software interface, and versatility across various research fields.

“Having the CIQTEK SEM4000Pro available in our showroom allows us to showcase its imaging performance directly to our customers,” said a representative from SYNERGIE4. “It’s a great addition to our demonstration facilities and an important step in expanding our microscopy portfolio.”

With the SEM4000Pro now available in France, European users can directly evaluate its performance, supported by SYNERGIE4’s local expertise and technical demonstration services. This collaboration marks a significant milestone in CIQTEK’s ongoing effort to enhance accessibility to advanced electron microscopy technologies across Europe.

• Comprehensive Portfolio Displayed
  We presented flagship systems in electron microscopy (FIB/SEM, TEM), nuclear magnetic resonance (NMR) spectrometers, and BET surface area & porosimetry analyzers—underscoring our commitment to advancing analytical science.

• Integration of Oilfield Solutions under the QOILTECH Brand
  Under our specialized QOILTECH line, we introduced tools for petroleum exploration, including RSS, MWD/LWD systems, and near-bit gamma tools. These offerings were well received by participants seeking robust instrumentation for extreme environments.

• Strong Engagement & Feedback
  At the booth, we addressed technical queries and shared success stories from across the research and industry sectors. Many attendees expressed interest in follow-up collaborations, demos, and trial opportunities.

• Global Networking & Partnerships
  ARABLAB 2025 brought together distributors, end-users, and scientific institutions from across the world. CIQTEK strengthened relationships and opened dialogues for future regional projects and partnerships in the Middle East and beyond

CIQTEK thanks all visitors, partners, and colleagues who joined us in Dubai!

We look forward to continued collaboration and impactful research ahead!